Two novel ferrocenylphenyl-containing amides have been synthesized by reaction of ferrocenylbencarboxylchloride and 1, 2-di-(o-aminophenoxy)ethane. A single crystal X-ray analysis shows that compound 3 crystallizes in the triclinic system, space group P-1, and compound 4 crystallizes in orthorhombic system, space group Pca21. There are intramolecular H-bonds in both the compounds, two H-bonds in compound 3 and one in compound 4. The dihedral angels of Cp-ring and phenyl ring range from 3.8° to 20.8°.
